|
|
Decision threshold and detection limit in low-levels of radioactivity measurements |
WANG Chuangao1, LUO Zhiping1, PANG Hongchao1, YIN Yunyun1, ZHENG Guowen1, XU Yongjun1, LOU Hailin1, WANG Zhongwen1, LI Ruirui1,2 |
1. China Institute of Atomic Energy, Beijing 102413 China;
2. Washington University School of Medicine |
|
|
Abstract Objective The calculation methods for decision threshold and detection limit of radioactivity measurement for low background were discussed.Methods Based on the data from 18 biological samples measured by Alpha spectrometer, formulas of decision threshold and detection limit given in RSG1.2(IAEA), NUREG 1576(USA)and AQ48(IAEA) were used and discussed.Results Parts of the results decided by these three kinds of formulas would be entirely different,which indicated that formulas of NUREG 1576 and AQ48 were much more conservative than the formulas of RSG1.2 for low background counts(as<100).Conclusion To ensure the reliability when judging the measured data, formulas of decision threshold and detection limit must be chosen according to the actual condition (such as background counts, background count time and gross count time, etc.), especially in low-level radioactivity measurements.
|
Received: 16 July 2018
|
|
|
|
|
[1] ISO 11929:2010 Determination of the characteristic limits (decision threshold, detection limit and limits of the confidence interval) for measurements of ionizing radiation-Fundamentals and application[J].
[2] Strom DJ, Maclellan JA. Evaluation of eight decision rules for low-level radioactivity counting[J].Health Physics,2001,81(1):27.
[3] Rigaud D. A proposed method to determine the decision level for radioactivity measurements[J].Health Physics,2003,85(2):140-149.
[4] Currie L A.On the detection of rare, and moderately rare, nuclear events[J].Journal of Radioanalytical and Nuclear Chemistry,2008,276(2):285-297.
[5] NUREG-1576:Multi-acency radiological laboratory analytical protocols manual[J].2004.
[6] IAEA Analytical Quality in Nuclear Applications Series No. 48:Determination and Interpretation of Characteristic Limits for Radioactivity Measurements[J].2017.
[7] ASTM C1284-10, Standard Practice for Electrodeposition of the Actinides for Alpha Spectrometry, ASTM International, West Conshohocken, PA, 2010[M].
[8] IAEA-RS-G-1.2 ASSESSMENT OF OCCUPATIONAL EXPOSURE DUE TO INTAKES OF RADIONUCLIDES[J]. 1999.
[9] Currie LA. Limits for qualitative detection and quantitative determination. Application to radiochemistry[J]. Analytical Chemistry, 1968, 40(3):586-93.
[10] Strom D J, STANSBURY P S. Minimum detectable activity when background is counted longer than the sample[J].Health Physics, 1992, 63(3):360.
[11] Brodsky A. Accuracy and detection limits for bioassay measurements in radiation protection. Statistical considerations[J].Oecologia, 1986, 152(2):335-43.
[12] ANSI/HPS N13.30-1996 Performance Criteria for Radiobioassay and the Multi-Agency Radiation Survey and Site Investigation Manual[J].1996.
[13] 潘自强. 辐射安全手册[M].北京:科学出版社, 2011.
[14] ANSI-HPS N13.30-2011 Performance criteria for radiobioassay[J]. |
|
|
|